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Synthesis, characterisation and properties of a crescent-shaped tetranuclear bis-dirhodium complex

✍ Scribed by Anne Petitjean; Jean-Marie Lehn; Richard G Khoury; André De Cian; Nathalie Kyritsakas

Publisher: Elsevier Science
Year: 2002
Tongue: English
Weight: 94 KB
Volume: 5
Category: Article
ISSN: 1631-0748
DOI: 10.1016/s1631-0748(02)01379-6

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## Abstract A new binucleating bis(terdentate) ligand, 3,5‐[3‐bis(2‐pyridyl)pyrazole‐1‐ylmethyl]pyrazole (HL^2^), was synthesized. Reaction of the deprotonated ligand L^2^ with hydrated Cu^II^ salts gives (μ‐pyrazolato)(μ‐hydroxido)‐bridged binuclear and tetranuclear complexes [L^2^Cu~2~(μ‐OH)(ClO~