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Synthesis and X-ray structural study of octa-coordinated hexafluoroacetylacetone hafnium(IV) complex

✍ Scribed by K. V. Zherikova; N. B. Morozova; I. A. Baidina; V. I. Alekseev; I. K. Igumenov

Publisher
SP MAIK Nauka/Interperiodica
Year
2006
Tongue
English
Weight
123 KB
Volume
47
Category
Article
ISSN
0022-4766

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Synthesis and structural investigation of hafnium(IV) complexes with acetylacetone and trifluoroacetylacetone
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Two volatile hafnium(IV) complexes with acetylacetone and trifluoroacetylacetone (HL) have been prepared and their structures have been studied at -30 . Crystal data for C 20 H 28 HfO 8 : a = 21.5493(4) Γ…, b = 8.36720(10) Γ…, c = 13.9905(3) Γ…; = 116.5550(10) , space group 2/c, Z = 4, d calc = 1.692 g