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Synthesis and X-ray Characterization of an Octaalkynyldibenzooctadehydro[12]-annulene

โœ Scribed by Tovar, John D.; Jux, Norbert; Jarrosson, Thibaut; Khan, Saeed I.; Rubin, Yves


Book ID
118266508
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
49 KB
Volume
63
Category
Article
ISSN
0022-3263

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Synthesis and X-Ray Characterization of
โœ Ganesh K Ramachandran; Jianjun Dong; Jason Diefenbacher; Jan Gryko; Robert F Mar ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 544 KB

We report on the synthesis and characterization of two silicon clathrates, Na 8 Si 46 and Na x Si 136 (x โ€ซุโ€ฌ 4+23), by powder X-ray di4raction, combined with Rietveld pro5le analysis. In Na 8 Si 46 , no deviation from the ideal stoichiometry is observed. In Na x Si 136 , systematic changes in X-ray