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Synthesis and thermotropic characterization of a homologous series of racemic β-d-glucosyl dialkylglycerols

✍ Scribed by David A Mannock; Morio Akiyama; Ruthven N.A.H Lewis; Ronald N McElhaney


Book ID
117047707
Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
327 KB
Volume
1509
Category
Article
ISSN
0005-2736

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## Abstract 2‐__O__‐GA~29~β‐D‐glucopyranoside (1e) and 13‐__O__‐GA~29~, β‐D‐glucopyr‐anoside (1h) were synthesized from GA~29~ methyl ester (1b). Their structures were confirmed by ^1^H NMR and GC‐MS. Likewise, [17‐^13^C,T~2~]‐labelled 1e and 1h could be obtained. From [17‐^13^C,T~2~]GA~20~ (2a) an