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Synthesis and thermal stability of nanocrystalline chromium disilicide

โœ Scribed by Jianhua Ma; Yunle Gu; Liang Shi; Luyang Chen; Zeheng Yang; Yitai Qian

Book ID
116597580
Publisher
Elsevier Science
Year
2004
Tongue
English
Weight
135 KB
Volume
376
Category
Article
ISSN
0925-8388

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โœ Timothy J. Trentler; R. Suryanarayanan; Shankar M.L. Sastry; William E. Buhro ๐Ÿ“‚ Article ๐Ÿ“… 1995 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 351 KB

Sonochemical co-reduction of MoC15 and SiC14 with NaK alloy in a hexane dispersion using 600 W. 20 kHz irradiation, followed by annealing at 900 ยฐC produces nanocrystalline MoSi 2 powders with ~ 90% yield. Consolidation by hot pressing at 1170 ยฐC, 140 MPa for 4 h gives a 78%-dense compact with 31 nm