## Abstract A novel synthesis of the title compound was achieved by direct animation using Vicarious Nucleophilic Substitution (VNS) methodology. Reaction of 1,1,1‐trimethylhydrazinium iodide with 3,5‐dinitropyrazole in DMSO produces 4‐amino‐3,5‐dinitro‐1__H__‐pyrazole as a 1:1 crystal solvate with
✦ LIBER ✦
Synthesis and thermal behaviors of 4-amino-3,5-dinitro-1H-pyrazole
✍ Scribed by Wang, Ying-Lei; Zhao, Feng-Qi; Ji, Yue-Ping; Pan, Qing; Yi, Jian-Hua; An, Ting; Wang, Wei; Yu, Tao; Lu, Xian-Ming
- Book ID
- 119263434
- Publisher
- Elsevier Science
- Year
- 2012
- Tongue
- English
- Weight
- 608 KB
- Volume
- 98
- Category
- Article
- ISSN
- 0165-2370
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## Abstract magnified image A regiospecific cyclization‐dehydration reaction of a 1‐[(4‐(__N__‐alkyl‐__N__‐(__tert__‐butyloxycarbony)amino)‐phenyl]‐4,4,4‐trifluorobutane‐1,3‐done with a 4‐aminosulfonyl‐, or 4‐methylsulfonyl‐, phenylhydrazine hydrochloride in refluxing ethanol proceeded with simult