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Synthesis and structures of 5(3H)-oxotetrahydro-1H-imidazo[4,5-c][1,2,5]thiadiazole 2,2-dioxides

✍ Scribed by G. A. Gazieva; A. N. Kravchenko; K. A. Lyssenko; R. G. Gaziev; O. V. Lebedev; N. N. Makhova


Book ID
106520956
Publisher
Springer
Year
2008
Tongue
English
Weight
474 KB
Volume
57
Category
Article
ISSN
1573-9171

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## Abstract (__R__)‐5‐(diallylamino)‐5,6‐dihydro‐4__H__‐imidazo[4,5,1‐__ij__]quinolin‐2(1__H__)‐one (__12b__) was prepared in 9% overall yield from 3‐aminoquinoline. Reaction of __12b__ in ethyl acetate with tritium gas in presence of a 5% platinum on carbon catalyst afforded a mixture of (__R__)‐5