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Synthesis and Structure of the First Lanthanide Complex with the Bridging, Antiaromatic 2,2′-Bipyridine Dianion: [{Yb(μ2-N2C10H8)(thf)2}3]

✍ Scribed by Igor L. Fedushkin; Tatyana V. Petrovskaya; Frank Girgsdies; Randolf D. Köhn; Mikhail N. Bochkarev; Herbert Schumann

Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
101 KB
Volume
38
Category
Article
ISSN
0044-8249

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Treating [Cp\*V(l-Cl) 2 ] 3 (Cp\* = C 5 Me 5 ) and [(2,6-i-Pr 2 C 6 H 3 N) 2 MoMe 2 ], respectively, with Me 3 SnF afforded the title compounds [Cp\*V(l-F) 2 ] 4 (1) and [(2,6-i-Pr 2 C 6 H 3 N) 2 MoF 2 ] ´THF ( 2). 1 has a tetrameric structure, in which four V atoms can be regarded as being arranged