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Synthesis and structure of hexa-p-acetamidophenoxycyclotriphosphazene

✍ Scribed by Chistyakov, E. M.; Filatov, S. N.; Kireev, V. V.; Lysenko, K. A.; Buzin, M. I.; Chuev, V. P.

Book ID
115317524
Publisher
Springer
Year
2012
Tongue
English
Weight
220 KB
Volume
82
Category
Article
ISSN
1070-3632

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The hexa-tert-butyl substituted hexa-peri-hexabenzocoronene was synthesized in an overall yield of 83 % from 4-tert-butylphenylacetylene. The key step was the oxidative cyclodehydrogenation of hexa(4-tert-butylphenyl)benzene with anhydrous FeCl 3 in CH 2 Cl 2. The high solubility of hexa-tertbutyl-h