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Synthesis and structure of Fe[C5(CH2Ph)5]2 and Lu(C8H8)[C5(CH2Ph)5]

✍ Scribed by Herbert Schumann; Christoph Janiak; Randolf D. Köhn; Jörg Loebel; Andreas Dietrich


Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
1012 KB
Volume
365
Category
Article
ISSN
0022-328X

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Syntheses and crystal structures of [(C6
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## CeH5CHzCsH4)2GdCl.THF]2 (1) and ( C ~H ~C H Z C ~H ~) ~E ~C I . T H F (2) were prepared by the reaction of LnC13 ( Ln=Gd, Er) with benzylcyclopentadienyl sodium in THF and characterized by elemental analysis, IR, 'H NMR, 13C NMR, MS and thermal gravimetry. The crystal structures of both compoun