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Synthesis and structure of disubstitutedcloso-decaborate anion derivatives Ph4P(2,6-B10H8O2CCH3) and 1,2-B10H8Phen with bifunctional O,O’- and N,N’-substituents

✍ Scribed by Safronova, E. F.; Avdeeva, V. V.; Polyakova, I. N.; Vologzhanina, A. V.; Goeva, L. V.; Malinina, E. A.; Kuznetsov, N. T.

Book ID
121594053
Publisher
Springer
Year
2013
Tongue
English
Weight
311 KB
Volume
452
Category
Article
ISSN
0012-5008

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Preparation, 11B NMR, Vibrational Spectra, and Crystal Structure of (P( C6H5)4)2(1,10-(O2N)2B10H8). -The title compound (I) is obtained in ≈7% yield in addition to the known compounds (PPh4)3(B10H9(NO)B10H9) (≈12%), (PPh4)(1-N2B10H9) (≈9%); and (PPh4)2(1-(O2N)B10H9) (22%) and separated by ion excha