Synthesis and Structure of a Novel Organic-Inorganic Hybrid Polyoxovanadate, [Ni(bpp)2]2(V4O12) (bpp=1,3-bi-4-pyridylpropane)
✍ Scribed by Li-Juan Zhang; Zheng-Jun Hu; Zhuo Zhang; Hong-You Guo
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- English
- Weight
- 130 KB
- Volume
- 25
- Category
- Article
- ISSN
- 0256-7660
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Bromohexyl)-3¢,4¢-ethylenedioxy)-2,2¢-bithiophene (3): Into a roundbottomed flask were introduced EDOT (5.9 g, 41.4 mmol) and 150 mL of tetrahydrofuran (THF). The mixture was cooled to ±40 C and butyllithium, 2.5 M in hexanes (19 mL, 47.5 mmol), was added rapidly. After 1 h stirring, tributyltin chl