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Synthesis and Structure of a 1,1‘-Diphospha[2]ferrocenophane

✍ Scribed by Deschamps, Eliane; Ricard, Louis; Mathey, François

Book ID
126922205
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
46 KB
Volume
20
Category
Article
ISSN
0276-7333

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HeteroC4lradialene / 1,2-Diphosphetane / Butadiene, 2,3-bis(chlorophosphanyl)-1,2-Diphosphetane 4, the first "1,2-diphospha[4]radialene", has been prepared in 83% yield by the reductive coupling reaction of 2,3-bis(chloroisopropylphosphanyl)butadiene 3a with lith-ium in THF. The X-ray crystal struct