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Synthesis and Structure of 7-Methyl- and 7-Phenyl-1,2,3,4-tetrahydro-1,4-diazepin-5-ones

✍ Scribed by Hofmann, Corris M.; Safir, S. R.

Book ID: 120328851
Publisher: American Chemical Society
Year: 1962
Tongue: English
Weight: 497 KB
Volume: 27
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01057a040

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## Abstract Fused tricyclic 7‐phenyl‐5__H__‐thizolo[5,4‐__e__]pyrrolo[1,2‐__a__][1,4]diazepin‐10(9__H__)one (**10**) was prepared by thermolysis of 2‐phenyl‐4‐(1‐pyrrolylmethyl)thiazole‐5‐carbonyl azide (**9**) in acetic acid. In addition, starting from **10**, 7‐phenyl‐5__H__‐thiazolo [5,4‐__e__][