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Synthesis and structure of 1,3-diselenol-2-selenone

✍ Scribed by R. N. Lyubovskaya; Ya. D. Lipshan; O. N. Krasochka; L. O. Atovmyan

Book ID: 112439343
Publisher: Springer
Year: 1976
Tongue: English
Weight: 214 KB
Volume: 25
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf00925645

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## Abstract The reaction of 2,5‐dimethyl‐3,4‐diselenocyanato‐1__H__‐pyrrole by NaBH~4~ or NaOCH~3~ led to tetraselenide **7** in quantitative yield. Treatment of protected tetraselenide **8** with LiAlH~4~ afforded the aluminum complex intermediate that was converted into pyrrole‐annelated 1,3‐dise