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Synthesis and structure of 1-oxo-1-chlorophospholenes

✍ Scribed by B. A. Arbuzov; O. A. Vizel'; Yu. Yu. Samitov; Yu. F. Tarenko

Book ID: 112432758
Publisher: Springer
Year: 1967
Tongue: English
Weight: 208 KB
Volume: 16
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf00906012

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## Abstract 1‐Oxo‐1,3‐dithiolane (4) and its __cis__‐ and __trans__‐2‐methyl (5,6), ‐4‐methyl (7,8) and ‐5‐methyl (9,10) derivatives were prepared by oxidizing the corresponding 1,3‐dithiolanes (1–3) with NaIO~4~ in water. The oxides were purified and their isomers separated using thin layer chroma