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Synthesis and structure determination of 2,3-diaryl-9,9-dioxo-1H-9-thia-1,4,4a,7,10-pentaazaphenanthrene-2-ols

✍ Scribed by Sławiński, Jarosław; Pogorzelska, Aneta; Żołnowska, Beata; Laskowski, Tomasz; Sowiński, Paweł


Book ID
120934303
Publisher
Elsevier Science
Year
2013
Tongue
French
Weight
695 KB
Volume
69
Category
Article
ISSN
0040-4020

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The title compound, C 21 H 20 ClN 3 O 2 , was synthesized by the reaction of 4-chlorobenzaldehyde and 3-(5,5-dimethyl-3-oxocyclohex-1-enylamino)propanoic acid with malononitrile in ethylene glycol under microwave irradiation. The dihydropyridine ring has a boat conformation. The pyrimidine ring adop