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Synthesis and structural study of a new iron phosphate K3Fe(PO4)2

✍ Scribed by Besma Lajmi; Mourad Hidouri; Abdel-Karim Ben Hammouda; Alain Wattiaux; Léopold Fournés; Jacques Darriet; Mongi Ben Amara

Book ID: 113782812
Publisher: Elsevier Science
Year: 2009
Tongue: English
Weight: 620 KB
Volume: 113
Category: Article
ISSN: 0254-0584
DOI: 10.1016/j.matchemphys.2008.07.064

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## Abstract A single crystal of the new title compound is synthesized in a flux of Rb~2~Mo~2~O~7~ from a starting mixture of Rb~2~CO~3~, Fe(NO~3~)~3~, (NH~4~)~2~HPO~4~, and MoO~3~ (Pt crucible, 473, 673, and 873 K for 24 h at each temperature).