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Synthesis and structural diversity of lanthanide amidate complexes and their catalytic activities for the ring-opening polymerization of rac-lactide

✍ Scribed by Hu, Xiaolin; Lu, Chengrong; Wu, Bing; Ding, Hao; Zhao, Bei; Yao, Yingming; Shen, Qi

Book ID: 120218738
Publisher: Elsevier Science
Year: 2013
Tongue: English
Weight: 797 KB
Volume: 732
Category: Article
ISSN: 0022-328X
DOI: 10.1016/j.jorganchem.2013.02.022

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## Abstract Two methods to synthesize homoleptic guanidinate lanthanide complex are described. The samarium guanidinate complex [Sm{Ph~2~NC(NCy)~2~}~3~]·2C~7~H~8~ (1) can be synthesized by the metathesis reaction of lithium guanidinate with anhydrous samarium trichloride in a 3:1 molar ratio. The a