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Synthesis and Structural Characterization of Novel β-Tropolone Derivatives.

✍ Scribed by Vitalii N. Komissarov; Dyong Nghia Bang; Vladimir I. Minkin; Sergei M. Aldoshin; Valery V. Tkachev; Gennady V. Shilov

Publisher
John Wiley and Sons
Year
2004
Weight
77 KB
Volume
35
Category
Article
ISSN
0931-7597

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The titanocene vinylidene intermediate [Cp\* 2 Ti=C=CH 2 ] (9) The azatitanacyclobutane [Cp\* 2 Ti{ϪNPhϪC(Ph)(H)Ϫ(C= CH 2 )Ϫ}] (22) was formed from the reaction between 9 and reacted with the carbodiimides RϪN=C=NϪR [R = p-CH 3 C 6 H 4 (19a), C 6 H 11 (19b)] to give the N=C-cycloaddition benzylidene