Synthesis and structural characterization of In-doped ZnFe2O4 nanoparticles
β Scribed by M. Maletin; Evagelia G. Moshopoulou; A.G. Kontos; E. Devlin; A. Delimitis; V.T. Zaspalis; L. Nalbandian; V.V. Srdic
- Publisher
- Elsevier Science
- Year
- 2007
- Tongue
- English
- Weight
- 385 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0955-2219
No coin nor oath required. For personal study only.
β¦ Synopsis
In-doped ZnFe 2 O 4 nanoparticles were prepared by a co-precipitation method. The nanoparticles were charactarized by conventional powder Xray diffraction, energy dispersive X-ray spectrometry, transmission electron microscopy, Raman and MΓΆssbauer spectroscopy. It was found that Zn 1-x In x Fe 2 O 4 nanoparticles of size β4 nm can be formed for 0 β€ x β€ 0.6. However, only for 0 β€ x β€ 0.15, was it possible to obtain single phase samples. These new Zn 1-x In x Fe 2 O 4 (0 β€ x β€ 0.6) nanoparticles exhibit behavior distinct from their bulk counterparts and present an evolution of the structural and physical properties as a function of x. Detailed results, as well as the interest of these materials both for applied and basic science perspectives will be presented.
π SIMILAR VOLUMES
Mn 1Γx Zn x Fe 2 O 4 nanoparticles were prepared by hydrothermal synthesis at 200 1C for 12 h and characterized by X-ray powder diffraction (XRD), FESEM and vibrating sample magnetometer (VSM) techniques. The additions of Zn 2+ ions content reduced the nanoparticles size. With the increase of Zn 2+
Spinel-type (S.G. ΒΌ Fd3 Β―m) ZnFe 2 O 4 fine particles with sizes from 4 to 19 nm prepared by solvothermal and microwave-assisted solvothermal methods have been studied by neutron powder diffraction at room temperature. The cation distribution corresponding to mixed spinel structure (Zn x ]O 4 along