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synthesis and Structural Characterization of Homoleptic Gallium Amides

✍ Scribed by Atwood, David A.; Atwood, Vicki O.; Cowley, Alan H.; Jones, Richard A.; Atwood, Jerry L.; Bott, Simon G.

Book ID
127336208
Publisher
American Chemical Society
Year
1994
Tongue
English
Weight
466 KB
Volume
33
Category
Article
ISSN
0020-1669

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A new synthesis procedure is reported for the preparation of mixed Al,Ga-offretites over the entire solid solution range 0 5 Ga/(Ga + Al) I 1. The resulting materials are characterized by X-ray powder diffraction, adsorption microcalorimetry and multinuclear solid state NMR. The 29Si MAS-NMR data ar