Synthesis and structural characterization of dithiacyclophanes derived from biaryldithiols
β Scribed by Upul K. Bandarage; Lyall R. Hanton; Robin A.J. Smith
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- French
- Weight
- 766 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0040-4020
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The titanocene vinylidene intermediate [Cp\* 2 Ti=C=CH 2 ] (9) The azatitanacyclobutane [Cp\* 2 Ti{ΟͺNPhΟͺC(Ph)(H)Οͺ(C= CH 2 )Οͺ}] (22) was formed from the reaction between 9 and reacted with the carbodiimides RΟͺN=C=NΟͺR [R = p-CH 3 C 6 H 4 (19a), C 6 H 11 (19b)] to give the N=C-cycloaddition benzylidene
## Abstract A procedure is described to synthesize heterocyclic cyanuric acid based triglycidyl isocyanurate resin in good yield and purity. The purity and configuration of the resin were confirmed by determination of the melting point, IR and NMR spectroscopy, elemental analysis, and epoxide equiv