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Synthesis and Structural Analysis of Sr 5.8 La 4.4 Ti 7.8 S 24 O 4 and La 14 Ti 8 S 33 O 4 : Two New Oxysulfides Containing a Common [(Ti 4 S 2 O 4 )(TiS 6 ) 4/2 ] 12- Layer

โœ Scribed by Tranchitella, Louis J.; Fettinger, James C.; Eichhorn, Bryan W.


Book ID
126332658
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
206 KB
Volume
8
Category
Article
ISSN
0897-4756

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Synthesis and Structure Determination of
โœ L Cario; C Deudon; A Meerschaut; J Rouxel ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 714 KB

The new compound La 8 Ti 10 S 24 O 4 has been prepared from a mixture of La 2 Ti 2 O 7 and La 2 O 3 (in a 5:1 ratio) heated at 1200ยฐยฐC under a H 2 S gas flow. This new quaternary phase was obtained due to an incomplete sulfidizing process. Single-crystal X-ray diffraction studies show that La 8 Ti 1