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Synthesis and Stereochemical Aspects of Ethyl 1,1a,2,3,4,5,6,6a-Octahydro-4-octylcyclopropa[f]indene-1-carboxylate

✍ Scribed by Zakir Hussain; Debasis Koley; Henning Hopf

Publisher: John Wiley and Sons
Year: 2005
Tongue: German
Weight: 188 KB
Volume: 88
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.200590262

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✦ Synopsis

Abstract

A novel approach for the synthesis of carbene adducts 9a/9b and 10/11 is reported. Identification of the geometric and positional isomers of carbene addition was carried out by reversed‐phase HPLC, and the establishment of the structure and configuration of 9a/9b was performed by means of 2D‐NMR.

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