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Synthesis and spectroscopic properties of some di- and trideuterated methylpyridines

✍ Scribed by James W. Pavlik; Tharinee Vongnakorn; Supawan Tantayanon

Publisher
Journal of Heterocyclic Chemistry
Year
2009
Tongue
English
Weight
86 KB
Volume
46
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

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2‐Trideuteriopyridine‐4,6‐d~2~ (1‐4,6‐d~2~), 3‐methylpyridine‐2,6‐d~2~ (2‐2,6‐d~2~), 3‐methylpyridine‐2,4,6‐d~3~ (2‐2,4,6‐d~3~), and 4‐trideuteriopyridine‐2,6‐d~2~ (3‐2,6‐d~2~) were synthesized from the appropriate 2‐, 3‐, or 4‐methylpyridine N‐oxides. These deuterated products were characterized by their ^1^H NMR and ^13^C NMR spectra. J. Heterocyclic Chem., 46, 213 (2009).

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