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Synthesis and Spectroscopic Characterization of Ethylidynearsine

✍ Scribed by Guillemin, Jean-Claude; Lassalle, Laurent; Drean, Pascal; Wlodarczak, Georges; Demaison, Jean

Book ID: 126807340
Publisher: American Chemical Society
Year: 1994
Tongue: English
Weight: 882 KB
Volume: 116
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00099a010

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## Abstract Hydrolysis of 3β‐5‐diacetoxy‐5β‐cholestan‐6‐one oxime (1) gave seven products which, in addition to 3β‐acetoxy‐ and (6__E__)‐3β‐hydroxy‐5‐methoxy‐5α‐cholestan‐6‐one oxime (3 and 4), are identified as the dimeric steroids (6__E__,6′__E__)‐6‐(6′‐hydroxyimino‐5′α‐cholestan‐5′‐yl‐oximino)ch