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Synthesis and Self-Assembly of Functionalized Hexa-peri-hexabenzocoronenes

✍ Scribed by Shunji Ito; Mike Wehmeier; J. Diedrich Brand; Christian Kübel; Rebekka Epsch; Jürgen P. Rabe; Klaus Müllen

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
312 KB
Volume
6
Category
Article
ISSN
0947-6539

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Synthesis and Structural Characterizatio
Synthesis and Structural Characterization of Hexa-tert-butyl- hexa-peri-hexabenzocoronene, Its Radical Cation Salt and Its Tricarbonylchromium Complex
✍ Peter T. Herwig; Volker Enkelmann; Oliver Schmelz; Klaus Müllen 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 369 KB 👁 2 views

The hexa-tert-butyl substituted hexa-peri-hexabenzocoronene was synthesized in an overall yield of 83 % from 4-tert-butylphenylacetylene. The key step was the oxidative cyclodehydrogenation of hexa(4-tert-butylphenyl)benzene with anhydrous FeCl 3 in CH 2 Cl 2. The high solubility of hexa-tertbutyl-h