The thermally induced formation of methyl-and phenylthiohydantoin amino acid derivatives from the corresponding N-methyl-and N-phenylthiourea derivatives of amino acids and peptides has been shown to occur in the mass spectrometer. A comparison of the mass spectra of a number of amino acid thiourea
Synthesis and quantitation of glucitollysine, a glycosylated amino acid elevated in proteins from diabetics
✍ Scribed by Beat Trüeb; Graham J. Hughes; Kaspar H. Winterhalter
- Publisher
- Elsevier Science
- Year
- 1982
- Tongue
- English
- Weight
- 401 KB
- Volume
- 119
- Category
- Article
- ISSN
- 0003-2697
No coin nor oath required. For personal study only.
✦ Synopsis
A method for preparative synthesis of glucitollysine in high yield is described.
It is shown that this compound is useful as a standard for the determination of nonenzymatic glycosylation of proteins.
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