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Synthesis and Protection of Aryl Sulfates Using the 2,2,2-Trichloroethyl Moiety.

✍ Scribed by Yong Liu; I-Feh Felicia Lien; Scott Ruttgaizer; Peter Dove; Scott D. Taylor


Publisher
John Wiley and Sons
Year
2004
Weight
184 KB
Volume
35
Category
Article
ISSN
0931-7597

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A series of 1-(perfluoroalkanesulfonylamino)-2,2,2-(trichloroethyl)dialkylphosphonates R f SO 2 NHCH-(CCl 3 )P(O)(OR) 2 has been synthesized in good yields by addition of dialkyl phosphite to N-perfluoroalkanesulfonyltrichloroaldimines R f SO 2 N‫ב‬CHCCl 3 that were prepared by treatment of N,N-dich