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Synthesis and properties of 5-alkynyl-1,2,3-triazoles

✍ Scribed by I. N. Domnin; L. A. Remizova; G. L. Starova; F. Rominger

Book ID
111465198
Publisher
SP MAIK Nauka/Interperiodica
Year
2009
Tongue
English
Weight
377 KB
Volume
45
Category
Article
ISSN
1070-4280

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Herein we report an approach to the formation of 5-alkynyl-1,3-dioxin-4-ones using Suzuki-Miyaura cross-coupling reaction of potassium alkynyltrifluoroborate salts with 2,2,6-trimethyl-5-iodo-1,3dioxin-4-one. The resulting 5-ethynyltrimethylsilyl-1,3-dioxin-4-ones obtained through the Sonogashira re

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## Abstract Optimized conditions are applied to the Suzukiβ€”Miyaura cross‐coupling of potassium alkynyl trifluoroborates with the iodinated 1,3‐dioxin‐4‐one (I).