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Synthesis and properties of [2.2](3,3′)biphenylo(3,6)phenanthrenophane

✍ Scribed by Yosuke Nakamura; Tadahiro Mita; Jun Nishimura

Book ID
103405997
Publisher
Elsevier Science
Year
1996
Tongue
French
Weight
225 KB
Volume
37
Category
Article
ISSN
0040-4039

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with the DessNartin periodinane (1) in fluorotrichloromethane (freon 11). Use of the freon solvent greatly improved the recovery of this volatile aldehyde. Similarly the oxidation of 3,4-2Hz-3Z-hexen-1-ol (5) yielded 3,4-'HZ- 3Z-hexenal (6) in a 92% isolated yield with a purity of greater than 99%.