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Synthesis and properties of 1,3-dithiole-[3]- and [4]-dendralenes, acyclic systems of the corresponding [3]- and [4]-radialenes

✍ Scribed by Yohji Misaki; Yasushi Matsumura; Toyonari Sugimoto; Zen-ichi Yoshida

Book ID: 104244850
Publisher: Elsevier Science
Year: 1989
Tongue: French
Weight: 299 KB
Volume: 30
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)93767-0

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✦ Synopsis

1,3-Dithiole-[3]-and [4]-dendralenes (2 and 3) have successfully been synthesized by using Vilsmeyer reactions on 2,2'-(ethanediylidene)bis(l,3-dithiole) (5) and 2 and the following Wittig reaction, Their electrochemical properties are discussed in comparison with those of 2 and 1,3-dithioleI4lradialene (4). Furthermore, conversion of 2 and 2 to 1,3-dithiole-[3]radiaIene and 4, respectively, was attempted by using zero-valent nickel complexes.

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