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Synthesis and polymorphism of deuterium labeled unsaturated monogalactosyl diglyceride as studied by 2H NMR

✍ Scribed by Vladimir Chupin; Svetlana Smirnova; Ben de Kruijff


Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
394 KB
Volume
113
Category
Article
ISSN
0165-0513

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✦ Synopsis


Abstract

The synthesis and polymorphism of deuterium‐labeled 1,2‐di‐O‐[11‐^2^H~2~)‐oleoyl]‐3‐O‐β‐D‐galactopyranosyl)‐rac‐glycerol is described. ^2^H‐NMR studies show that this lipid in its hydrated state adopts a lamellar phase below ‐ 5°C and an inverted hexagonal phase above ‐ 5°C.