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Synthesis and optoelectronic properties of transition metal complexes incorporating dithieno[3,2-b:2′,3′-d]phosphole ligands

✍ Scribed by Dienes, Yvonne ;Eggenstein, Matthias ;Neumann, Toni ;Englert, Ulli ;Baumgartner, Thomas


Book ID
120254454
Publisher
Royal Society of Chemistry
Year
2006
Tongue
English
Weight
280 KB
Volume
11
Category
Article
ISSN
1477-9226

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A convenient and improved synthesis of d
✍ Fredrik Allared; Jonas Hellberg; Tommi Remonen 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 52 KB

An improved synthesis of dithieno[3,2-b:2%,3%-d]thiophene 1 is presented. By starting from 2,3-dibromothiophene 2 the total yield was improved from 35 to 58%. We also describe a more convenient synthesis of one of the reagents, benzenesulfonic acid thioanhydride 3.