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Synthesis and NMR Studies of 13 C-Labeled Vitamin D Metabolites 1

โœ Scribed by Okamura, William H.; Zhu, Gui-Dong; Hill, David K.; Thomas, Richard J.; Ringe, Kerstin; Borchardt, Daniel B.; Norman, Anthony W.; Mueller, Leonard J.


Book ID
121389347
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
199 KB
Volume
67
Category
Article
ISSN
0022-3263

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Natural Abundance 13C-NMR. of Vitamin D3
โœ Thomas H. Williams; David N. Greeley; Enrico G. Baggiolini; John J. Partridge; S ๐Ÿ“‚ Article ๐Ÿ“… 1980 ๐Ÿ› John Wiley and Sons ๐ŸŒ German โš– 312 KB

## Abstract Chemical shifts of ^13^Cโ€ and ^1^Hโ€NMR. spectra of vitamin D~3~ metabolites (**2โ€“7**) are assigned. Substituent effect parameters due to hydroxyl groups are deduced by comparison with vitamin D~3~.