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Synthesis and NMR spectroscopic characterization of Si-substituted 1-silacyclobutene derivatives

✍ Scribed by Khan, Ezzat ;Wrackmeyer, Bernd

Book ID: 111488174
Publisher: Walter de Gruyter GmbH
Year: 2011
Tongue: English
Weight: 595 KB
Volume: 9
Category: Article
ISSN: 2391-5420
DOI: 10.2478/s11532-010-0122-z

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## Abstract The reaction of di(alkyn‐1‐yl)silanes Me(R)Si(CC^__t__^Bu)~2~ [1; R = Me (a), H (b)] with diethylborane or 9‐borabicyclo[3.3.1]nonane in a 1 : 1 ratio affords the 1‐silacyclobutene derivatives 6a, 7a,b as a result of intermolecular 1,1‐hydroboration followed by intramolecular 1,1‐organ