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Synthesis and ionic hydrogenation of 1,1-phthaloyl-2-phenyl-3-(p-Alkylbenzoyl)cyclopropanes

โœ Scribed by S. I. Belykh; G. A. Kudryavtseva; N. M. Loim; L. P. Zalukaev; Z. N. Parnes; D. N. Kursanov

Book ID
112441920
Publisher
Springer
Year
1978
Tongue
English
Weight
390 KB
Volume
27
Category
Article
ISSN
1573-9171

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E-(S)-(1-Dimethoxyphosphoryl-2-phenyl)vinyl p-tolyl sulfoxide 3 was found to undergo cyclopropanation with sulfur ylides [dimethyl(oxo)sulfonium methylide, diphenyl sulfonium isopropylide and ethyl (dimethylsulfuranylidene)acetate (EDSA)] in a highly diastereoselective manner. The major diastereomer