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Synthesis and Evaluation of Boronated Lysine and Bis(carboranylated) γ-Amino Acids as Monomers for Peptide Assembly

✍ Scribed by Christophe Morin; Christian Thimon

Publisher: John Wiley and Sons
Year: 2004
Tongue: English
Weight: 144 KB
Volume: 2004
Category: Article
ISSN: 1434-193X
DOI: 10.1002/ejoc.200400342

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✦ Synopsis

Abstract

We have synthesized N‐Fmoc amino acid derivatives bearing boronated and carboranylated substituents. Thus, a 1,3,2‐dioxaborolane subunit has been introduced on the side chain of N^α^‐Fmoc‐L‐lysine, and a bis(carboranylated) γ‐amino acid building block has been prepared. As shown by the preparation of a model tetrapeptide, only the latter monomer can be successfully used in peptide synthesis. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)

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