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Synthesis and crystallographic characterization of [Cd(OH2)2(μ-Br)4(Cd(2-hydroxyethyl sulfide) (μ-Br))2]n

✍ Scribed by Robin D. Rogers; Andrew H. Bond; Salvador Aguinaga

Book ID
105112883
Publisher
Springer
Year
1993
Tongue
English
Weight
455 KB
Volume
23
Category
Article
ISSN
1572-8854

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Synthesis and structural characterization of a face-sharing bioctahedral complex [HB(Me2Pz)3)BH][Br3Mo(μ-Br)3MoTp*] and an edge-sharing tetramolybdenum complex [Mo4(μ3-O)2(μ2-O)2(μ2-OH)2(O)4(Me2PzH)6](Br)4(Me2PzH2)2 (Tp*=hydridotris(3,5-dimethylpyrazolyl)borate); Pz=pyrazolyl)
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From a solution prepared by a reaction of Mo 2 (O 2 CCH 3 ) 4 with KTp\* (Tp\*= hydridotris(3,5-dimethylpyrazolyl)borate, HB(Me 2 Pz) 3 ), in diglyme at room temperature followed by addition of excess (CH 3 ) 3 SiBr to the red solution in refluxing THF, the complexes [HB(Me 2 Pz) 3 )BH][Br 3 Mo(m-Br