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Synthesis and Crystal Structures of Two Polymorphs of Trilanthanum Iridium Septaoxide (La3IrO7)

✍ Scribed by Rachel C. Severance; Adam H. Fox; Samuel J. Mugavero; Mark D. Smith; Hans-Conrad zur Loye

Publisher
Springer
Year
2010
Tongue
English
Weight
423 KB
Volume
41
Category
Article
ISSN
1572-8854

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Two polymorphs of Li 2 CuZrO 4 have been synthesized and their structures characterized by X-ray, neutron and electron diffraction. Both have novel types of ordered rock salt structure. b-Li 2 CuZrO 4 is tetragonal, a=4.165(1) ( A, c=9.418(1) ( A, I-4m2, Z=4, R I =5.9%; the four sets of octahedral s