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Synthesis and crystal structures of new mixed-valence terbium (III/IV) fluorides with a random distribution between Tb3+ and Tb4+

✍ Scribed by M. Josse; M. Dubois; M. El-Ghozzi; D. Avignant

Book ID: 116597530
Publisher: Elsevier Science
Year: 2004
Tongue: English
Weight: 306 KB
Volume: 374
Category: Article
ISSN: 0925-8388
DOI: 10.1016/j.jallcom.2003.11.140

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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During a phase relationship study of the system KF-TbF 3 -TbF 4 , carried out using X-ray diffraction on samples synthesized under a fluorine atmosphere, a new mixed-valence terbium fluoride, KTb 3 F 12 , was brought out. Its crystal structure was determined from single-crystal X-ray diffraction dat