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Synthesis and crystal structure of the perchlorate salt of diprotonated N,N′-bis(1-methylimidazole-2-methyl)1,5-diazacyclooctane

✍ Scribed by Miao Du; Xian-He Bu; Qiang Xu; Zhi-Liang Shang; Ruo-Hua Zhang

Book ID
110300175
Publisher
Springer
Year
2000
Tongue
English
Weight
61 KB
Volume
30
Category
Article
ISSN
1572-8854

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In a facile carbon-acid condensation reaction of bis(2-aminomethylpyridine)copper(II) with nitroethane and formaldehyde in basic MeOH the N,N' -bis(2-pyridylmethylene)-l,3-diamino-2-methyl-2-nitropropane)copper~I~) cation is produced in essentially quantitative yield. The perchlorate salt crystalliz