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Synthesis and crystal structure of Pr(mpo)3(DMSO)2(Hmpo = 2-mercaptopyridine N-oxide)

✍ Scribed by De-Zhong Niu; Lai-Long Mu; Zai-Sheng Lu; Bao-Ling Song; Bai-Wang Sun

Book ID
111591753
Publisher
Springer
Year
2004
Tongue
English
Weight
176 KB
Volume
34
Category
Article
ISSN
1572-8854

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## Abstract Pyridine‐2‐(3′‐mercaptopropanoic acid)‐__N__ ‐oxide (I), is a higher homologue of 1‐oxopyridinium‐2‐thioacetic acid (II) [1]. It crystallizes in monoclinic space group P2~1~ with a = 9.2168(2) Å, b = 4.1423(2) Å, c = 11.3904(4) Å, β = 98.65(2)°, V = 429.93(3) Å^3^ and Z = 2. The least‐s