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Synthesis and Crystal Structure of a Bis[6.3.3]propellane

✍ Scribed by Jamrozik, Janusz ;Żeslawski, Wojeciech ;Grochowski, Jacek ;Serda, Pawel ;Dauter, Zbigniew

Publisher: John Wiley and Sons
Year: 2006
Tongue: English
Weight: 257 KB
Volume: 1996
Category: Article
ISSN: 0947-3440
DOI: 10.1002/jlac.199619960416

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✦ Synopsis

Abstract

The bis[6.3.3]propellane 6 derivative of 2,2′,6,6′‐tetramethylbiphenyl was, in the final stage, synthesized by dehydration, of octaalcohol 5. X‐ray structure analysis revealed the highly symmetric shape of the molecule and disordered oxygen atoms in the tetrahydrofuran rings. The dihedral angle between LSQ phenyl planes is 62.6(1)°.

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