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Synthesis and crystal structure of 2′-(3,5-dioxo-1,2,4-triazinane-1-yl)acetic acid and the product of its reaction with copper(II) chloride

✍ Scribed by I. G. Filippova; O. A. Bologa; Yu. A. Simonov; M. Gdaniec; N. V. Gerbaleu


Publisher
SP MAIK Nauka/Interperiodica
Year
2005
Tongue
English
Weight
124 KB
Volume
31
Category
Article
ISSN
1070-3284

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Acetal-protected (2,4-dioxocyclohex-1-yl)acetic acid derivatives were prepared by the allylation of dilithiated 1,3-cyclohexane-1,3diones, by the protection of the carbonyl groups and by the oxidation of the alkene. The products were then transformed, by amide formation and subsequent cyclization, i