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Synthesis and chemical transformations of 2-cyclopropyl-2-diazoacetates

✍ Scribed by V. V. Prokopenko; G. P. Okonnishnikova; I. P. Klimenko; E. V. Shulishov; Yu. V. Tomilov

Publisher
Springer
Year
2007
Tongue
English
Weight
443 KB
Volume
56
Category
Article
ISSN
1573-9171

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Synthesis of cyclopropyl cyanide-2,2-d2
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✍ William B. Edwardsiii; David F. Glenn πŸ“‚ Article πŸ“… 1976 πŸ› John Wiley and Sons 🌐 French βš– 268 KB

## Abstract A convenient method for the synthesis of cyclopropyl cyanide‐2,2‐d~2~ has been elaborated. Reduction of methyl 3‐cyanopropionate with lithium borodeuteride followed by reaction of the resulting alcohol with triphenylphosphine and carbon tetrachloride gave 4‐chlorobutyronitrile‐4,4‐d~2~.