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Synthesis and Characterization of β-Cyclodextrin Bonded Metal Porphyrins

✍ Scribed by Zao-Ying Li; Cong Li; Jia-Feng Li

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
289 KB
Volume
20
Category
Article
ISSN
0256-7660

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✦ Synopsis

Abstract

Reactions of 5‐(p‐aminophenyl)‐10,15,20‐triphenyl porphyrin (1) with Ru~3~(CO)~12~ or M(OCOCH~3~)~2~ (M= Ni, Mn) afforded metalloporphyrins (4–6), respectively. 6‐Deoxy‐6‐iodo‐β‐cyclodextrin (2) and mono(6‐O‐trifluoromethanesulfonyl) permethylated β‐cyclodextrin (3) reacted with complexes 4–6 to give β‐cyclodextrin bonded metal porphyrins (7–9) and permethylated β‐cydodextrin bonded metal porphyrins (10–12) respectively. These new complexes were identified by MS, IR, UV‐visible and ^1^H NMR spectra, and elemental analysis.

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