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Synthesis and Characterization of Tetrakis[bis(trimethylsilyl)methyl]disilene

✍ Scribed by Prof. Dr. Satoru Masamune; Dr. Yuichi Eriyama; Dr. Takeshi Kawase

Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
266 KB
Volume
26
Category
Article
ISSN
0044-8249

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Tetrakis(trimethysilyl)phthalocyaninatoruthenium(II) (5) has been synthesized via the biaxially coordinated ((CH 3 ) 3 Si) 4 PcRu(3-Clpy) 2 (2) complex by thermal decomposition of the axial ligands of 2. ((CH 3 ) 3 Si) 4 PcRu (5) was characterized by NMR, IR and UV-vis spectroscopy and elemental ana