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Synthesis and characterization of some novel macrocyclic NiIIcomplexes

✍ Scribed by Najlaa S. Al-Radadi; Sawsan M. Al-Ashqar; Mohsen M. Mostafa

Publisher: Springer Netherlands
Year: 2010
Tongue: English
Weight: 392 KB
Volume: 69
Category: Article
ISSN: 0923-0750
DOI: 10.1007/s10847-010-9826-0

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## Abstract The condensation of bis(__o__‐formylphenyl) selenide with 1,2‐diaminoethane or 1,3‐diaminopropane yielded the new macrocyclic ligands 1 and 2 in very good yields. Crystals of 1 are monoclinic, space group __P__2~1~/__c__ with __a__ = 10.0648(10) Å, __b__ = 37.390(4) Å, __c__ = 8.0073(11